دانلود کتاب LC-NMR: Expanding the Limits of Structure Elucidation 2nd Edition
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توضیحات کتاب:
The much-anticipated second edition provides guidance in setting up LC-NMR systems, discussion of LC methods that are compatible with NMR, and an update on recent hardware and software advances for system performance, such as improvements in magnet design, probe technology, and solvent suppression techniques that enable unprecedented mass sensitivity in NMR. This edition features methods to quantify concentration and assess purity of isolated metabolites on the micro scale and incorporates computational approaches to accelerate the structure elucidation process. The author also includes implementation and application of qNMR and automated and practical use of computational chemistry combined with QM and DFT to predict highly accurate NMR chemical shifts. The text focuses on current developments in chromatographic-NMR integration, with particular emphasis on utility in the pharmaceutical industry. Applications include trace analysis, analysis of mixtures, and structural characterization of degradation products, impurities, metabolites, peptides, and more. The text discusses novel uses and emerging technologies that challenge detection limits as well future directions for this important technique. This book is a practical primary resource for NMR structure determination―including theory and application―that guides the reader through the steps required for isolation and NMR structure elucidation on the micro scale.
Contents: فهرست فصول
Chapter 1 Introduction to LC-NMR
Chapter 2 NMR Theory
Chapter 3 Separation Methods
Chapter 4 NMR Instrumentation and Probe Technologies
Chapter 5 NMR-Associated Isolation Technologies
Chapter 6 NMR Experiments
Chapter 7 Applications
Chapter 8 Other Specialized Flow NMR
Chapter 9 Quantitation of Isolated Compounds
Chapter10 QM/DFT Chemical Shift Prediction
پشتیبان: 09378828643
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